Back to Sam's
Laser FAQ Table of Contents.
Amateur Laser Construction
Sub-Table of Contents
Back to Sam's
Laser FAQ Table of Contents.
Back to Amateur
Laser Construction Sub-Table of Contents.
Introduction to Amateur Laser Construction
In
this chapter and the one that follows, we provide basic information on the
construction of various types of lasers from scratch.
Extensive basic information is provided on home-built laser safety, setting
up a home laser lab, sources of supplies and chemicals, vacuum systems, glass
working, structural materials, power supplies, and more.
Then, a variety of specific types of home-built lasers are described in more
detail. Much of this material is derived from the Scientific American collection
"Light and its Uses" [5] and from the email, Web sites, articles, and
experiences of those who have been successful in building their own lasers from
basic components and getting them to work (not taking the easy way out and using
commercial tubes or laser diodes!) - or have given it their best shot trying!
While this will not substitute the hands-on
of actually having built one of these lasers or detailed construction plans, it
may provide the spark to get you started!
First, let
us consider some ill-posed justifications for attempting to build a laser from
(almost) raw materials:
- Something can be put together quickly. Forget it. Any of the types of
lasers considered in this discussion will require many many hours, more like
months, to locate the materials, chemicals, and other supplies and to
construct, align, and get working - if you ever succeed at all.
Furthermore, you will be CONSTANTLY fiddling with adjustments like gas
fill, mirror alignment, power supply voltage/current. In many cases, total
laser lifetime is often short (a few hours) before a total rebuild is needed.
These are not generally set-it-and-forget-it type equipment! If you just want
a working laser, this is definitely NOT the way to go.
- Lasers are SO expensive. Yes in many cases, but what you get is something
that works (relatively) reliably with (relatively) minimal fiddling with
adjustments. In the end, you will likely spend more than you might think based
on your initial estimates simply because you cannot go and buy just the
quantity of materials or chemicals that you will need - 1 screw or 2 inches of
pyrex glass 5 mm ID tubing or 6 feet of #24 magnet wire, for example.
A $25 1 mW helium-neon laser and power supply, or $19.95 diode laser type
laser pointer may be satisfactory for your needs. These will be even less
expensive if you build your own power supplies - and orders of magnitude
easier than building an entire laser from scratch.
If these are
your only reasons for wanting to do this, you will rapidly tire of the endeavor
and the parts will end up in a box alongside that dusty old partially ground
telescope mirror you also never completed :-(.
However, there
are many justifications for embarking on an adventure of this type:
- Educational experience. I guarantee that you will learn a tremendous
amount in the process - even if your baby never actually produces a beam. You
will need to deal with a variety of disciplines (depending on the type of
laser) possibly including: glass working, vacuum and gas supply systems,
machining, design of high voltage power supplies, optical alignment, sensors,
and more. The effort and contact with multiple discipline may stimulate
interests in other areas as well.
- Challenge. It probably goes without saying that the production of coherent
light - even if for a short time - from a totally homemade laser represents a
tremendous achievement with enormous satisfaction value. Why do people climb
mountains? Building a laser is like climbing from the depths of the Pacific to
the top of Everest and beyond. Note: If you don't believe this then you will
probably not have enough motivation to complete the project!
- Experimentation. There are many things you can try with full access to
both the inside and outside of the laser resonator that are impossible with a
sealed HeNe or Ar/Kr ion tube. Variations on the lasing medium including (for
gas lasers) the types and pressures of the gas fill or (for dye lasers), the
types and concentrations of dyes themselves; types of excitation (direct
discharge, RF, light); alternative optics like curved and plane mirrors,
prisms, lenses, and coatings,
Note: There may be
some reduncdancy with some of these photos as they may be present on multiple
locations including the Amateur Laser
Constructors Web site.
(From: Chris Chagaris (pyro@grolen.com)).
(From: Thieu Asselbergs
(asselber@fys.ruu.nl)).
(From: Laserist (laserist@geocities.com)).
These drawings show the structure and power supplies for some of
the lasers built by amateurs. These diagrams are based on the laser articles
from Scientific American (including the book: "Light and its Uses" - see the
section: Light and
its Uses - Table of Contents for an explanation as to why copies of or links
to the original artwork could not be provided). Their purpose is to give you a
flavor of what this type of laser construction entails - but are NOT intended as
dimensioned plans and are NOT drawn to scale. Refer to the more detailed
description in the chapter: Home-Built
Laser Types, Information, and Links and the relevant Scientific American
articles.
Start by locating back issues of Scientific American and/or
their reprint collections such as "Light and Its Uses" [5]. There have been many
practical articles and Amateur Scientist columns on lasers, laser construction,
and other laser related subjects, particularly during the initial laser craze of
the 1960s and 1970s but extending to the present particularly for more exotic
types of lasers and laser applications. A large public or university library
will likely have all of these somewhere though you may have to request them from
their storage vaults and/or they may be on microfilm or microfiche.
See the section: Light and
its Uses - Table of Contents for a list of all the articles that constitute
this valuable collection and an explanation of why I cannot provide on-line
access to it.
Here is a list of some of the laser articles that have been published in the
Amateur Scientist columns of Scientific American. The first 7 of these
constitute the chapters on laser construction found in "Light and its Uses":
- Helium-Neon Laser, September, 1964, pg. 227.
- More on the Helium-Neon Laser, December, 1965, pg. 106.
- Argon Ion Laser, February, 1969, pg. 118.
- Tunable Dye Laser, February, 1970, pg. 116.
- Carbon Dioxide Laser, September, 1971, pg. 218.
- Infrared Diode Laser, March, 1973, pg. 114.
- Nitrogen Laser, June, 1974, pg. 122.
- Mercury-Vapor Laser, October, 1980, pg. 204.
- Copper Chloride Laser, April, 1990, pg. 114.
Except for the one in
(6) which for all practical purposes you can ignore (it tells you how to hook up
a long obsolete type of laser diode), all the others are built from the ground
up using basic materials (i.e., glass tubing, pieces of plastic and metal,
mirrors and other optics, glue, duct tape, various bottled gasses and other
chemical supplies, high voltage transformers, resistors, capacitors, diodes,
wire, etc.).
As an aside, I lament the fact that few of the more recent Amateur Scientist
columns have nearly as much sophistication and depth as those from that era. On
the other hand, experiments that are presented may be performed by nearly anyone
who is reasonably handy using parts from the local home center and Radio Shack
and yet this is definitely real science. There is no need for high vacuum
systems, glass working skills, strange gas mixtures and other chemicals, or
fancy test equipment!
While the Scientific American Web site
has many interesting articles, they do not go far enough back to be of much use
for laser construction. There is an Index to the
Amateur Scientist articles maintained by the Society of Amateur Scientists (SAS) or
see the section: Light and
its Uses - Complete Table of Contents. However, the articles are not on-line
(see the explanation there of why this was not possible) so you still have to do
the leg-work!
The Society for Amateur Scientist
(SAS) Web site includes among other things, a technical forum devoted to the
interests of, you guessed it, amateur scientists like you:
Laser specific traffic on this forum
is quite small but the high chance of finding someone with similar interests
balances this out to some extent!
Check out the Amateur Laser
Constructors Web site and the other links to home-built lasers and related
projects in the section: Amateur
Laser Construction/Laser Communications Sites and Links to see what others
have done. Contact them via email. One thing is certain: since there are so few
hobbyist types interested in this sort of thing anymore, these people should
jump at any opportunity to discuss their passion to build lasers with you. The
site also has a variety of useful links and pointers to Scientific American and
other articles on lasers and related topics.
Information Unlimited has what are
supposedly complete plans argon ion, carbon dioxide, nitrogen, copper vapor, and
tunable dye lasers. (In the case of the CO2 laser, they have parts, kits, and
completely assembled versions as well - supposedly.) I doubt that it is
coincidental that these are also most of the types of lasers covered in the
Amateur Scientist columns of Scientific American! I do not know whether if the
plans are of any value beyond those or whether they are indeed just poor
reproductions or transcriptions. I also have no idea of whether what they
provide is credible for the price or whether it is likely to result in a
successfully completed project. Also see the section: Electronic
and Laser Project Parts, Plans, Specialized Components for additional
comments about Information Unlimited.
MWK Industries also has plans for
most of the types of lasers included in "Light and its Uses". As with the plans,
above, I do not know if these are derived from there or elsewhere or whether
there is any benefit to buying these as opposed to digging up the info in "Light
and its Uses" in conjunction with this document!
Thanks to Chris Chagaris (Email: pyro@grolen.com) for his comments and
additions to this document. His first-hand experience in constructing several
lasers from scratch has been extremely valuable in polishing and enhancing this
and the chapter on Home-Built
Laser Types, Information, and Links that follows.
Back to Amateur
Laser Construction Sub-Table of Contents.
Setting up a Home Laser Lab
There
are a variety of issues that are important for any sort of home lab or workshop
but the following, in particular, apply directly to lasers and laser
construction:
- Laser safety. In some ways, a homebuilt laser is MORE dangerous in terms
of risk to vision (at least) compared to a commercial one. One reason is that
the output power and behavior is less predictable - and there are no
manufacturer's specifications for MAXIMUM output. Therefore, one must err on
the side of caution - assume that they are at the upper end of any possible
range of power outputs. For all except the CO2 laser, these will at least be
well into the Class IIIb range. The CO2 WILL be Class IV! This doesn't mean
you will get an eye-killer beam from your laser - just that you cannot safely
assume you WON'T!
See the chapter: Laser
Safety for more information.
- High voltage. The power supplies for these lasers almost all involve high
voltage at significant current and/or with sizable high voltage filter or
energy storage capacitors.
- The neon sign/luminous tube transformers often used for excitation of
gas lasers come in various sizes but are all potentially lethal. The larger
ones, even more so.
- Any time you are storing energy in multi-KV storage capacitors, you are
talking about seriously deadly equipment.
- Even little high voltage inverters running off some AA batteries can
generate deadly output - especially where a capacitor is involved.
Read and understand the information in the document: "Safety Guidelines for
High Voltage and/or Line Powered Equipment" BEFORE constructing and powering
any of these systems.
- Water/liquids. The CO2 laser will require water cooling. You may want to
add water cooling to others like the Ar/Kr laser to boost output power. The
dye laser involves the use of liquids - some of them quite nasty. All use high
voltage AC line connected power supplies. This makes these doubly dangerous.
Make sure all precautions are taken including proper wiring and grounding of
all equipment AND plumbing! Even though the HV discharge is supposed to be
between special electrodes, it can jump to nearby metal fittings - and you!
- Vacuum vessels. The potential energy of the atmosphere working on a vacuum
is enormous. Every square inch of surface area separating the atmosphere from
an evacuated volume represents 14.7 pounds of force. A gallon jar with the air
pumped out may have over 1.5 TONS of force attempting to crush it. The results
of an implosion can be spectacular and are something you don't want to
experience first-hand.
Note that it is the difference between atmospheric pressure and that of
your vacuum that determines the stress on the container - whether you are
pumping down to 10 Torr or 1E-14 Torr is for all practical purposes irrelevant
with respect to implosion risk!
- Toxic/corrosive chemicals. Some of the materials used for glass cleaning,
electrode coatings, and organic dyes (for dye lasers) are extremely toxic,
corrosive, or both. Make sure you understand the chemical safety issues.
- Poisonous chemicals can get picked up on cleaning materials, clothing,
surfaces of lab glassware, tabletops, storage cabinets, the bottom of your
shoes, etc.
- The fumes from these chemicals are likely to be toxic and irritating as
well.
- Flammable or suffocating gasses. While the actual quantities of gasses
used in most of these lasers is infinitesimal (since they operate at a very
small fraction of atmospheric pressure), some gas will escape and leaks can
occur.
- These are all colorless and most are odorless so there will be no
visible signs of a leak or buildup of fumes.
- Proper ventilation must be provided
- Gasses that are heavier than air in particular can hang around resulting
in a layer that you cannot breath or one that is flammable.
- Glassworking, annealing, and outgassing flames. Needless to say, any time
that open flames are used, precautions must be taken to assure that no
flammable materials are in the vicinity.
- Obviously, this includes the chemicals and gasses mentioned above.
- Shavings from wood and plastic gutting, filing, grinding, and sanding
are extremely flammable and should be completely cleaned up and removed
before lighting the propane or oxy-hydrogen glass working torch!
- Have a fire extinguisher of the proper type - rated for chemical AND
electrical fires - in a location that is accessible outside the range of any
possible fire. Make sure you cannot be trapped by a fire. Two fire
extinguishers and two means of egress at opposite ends of the lab are even
better.
There didn't appear to be a critical mass of lawyers
present at the time most of the articles in "Light and its Uses" were written.
Therefore, they tend not to deal with the safety issues as emphatically as might
be desired. Most of these projects have aspects (most often the high voltage
power supplies) that are potentially dangerous or lethal. Safety must be at the
top of your list of priorities when undertaking such an endeavor!
Since any of
these lasers represents a long term comittment, it is essential that an area be
set aside for your laser lab. Therefore, the kitchen or dining room table is NOT
an appropriate place to be constructing a laser. It is possible to do without
the sort of setup depicted in the section: Possible
Laser Lab Layout but there are some basic requirements for a safe,
functional, and convenient space:
- An area that is as dust free as possible is absolutely essential. Dirt,
dust, condensed tobacco smoke or cooking grease, or other contamination of
optical surfaces is a major cause of problems in getting a laser to work
and/or result in reduced output power or erratic operation.
Forget about smoking around precision optics. Aside from slowly killing
yourself, a miniscule amount of tobacco smoke residue will play havoc with
mirrors and lenses - especially inside the laser resonator. You will be
wasting your time or worse. Just because you saw a demo where someone blew
smoke in the path of a laser beam to make it visible is no excuse as that was
just a one-time demo. There are special means of generating smoke for this
purpose which are non-toxic and do not condense on optical surfaces should a
real need arise.
- You must be able to leave it undisturbed probably for weeks or MONTHS on
end. Therefore, a spare room is best. You definitely don't want to share your
lab with a woodworking or gardening operation. Or, your kid brother who likes
to wreck EVERYTHING! :-)
- There must be access to electricity. A pair of dedicated circuits with
local cutoff switches/circuit breakers is nice. Install outlet strips all
along the walls behind your work surfaces.
- There probably needs to be running water and a drain. Where chemicals are
involved, the drain should be direct to a sewer, not a sump - assuming you can
safely put them down at all.
- There must be adequate ventilation. However, there should be NO way for a
laser beam to escape to the outside world! This means there can be no open or
uncovered windows! And, if your laser accidentally drills a hole through your
stone and stucco exterial wall, patch it up as quickly as possible. :-)
- Minimization of fire and water damage risk. This is mostly common sense
meaning a room with a concrete or vinyl floor and NO curtains or drapes. A
room in a dry basement is probably best if it can be made reasonably
dust-free.
- It must be large enough to provide space for you, the laser itself AND for
any additional length required by alignment or other optical add-ons to the
laser. Also, don't forget creature conforts for your guests like a sleep sofa
(for when you are performing critical mirror alignment), stereo, big screen TV
- OK, just kidding. ;-)
- Storage. There can never be too much. You need to be able to handle all
sorts of components, electronic and optical assemblies, partially or fully
completed lasers or other apparatus, chemicals, and other supplies.
- Metal double door supply cabinets are ideal for larger items and for
holding the multi-drawer parts cabinets you will also need (see below).
These are typically 18" to 24" deep by 36" wide and 60" to 78" tall with
multiple adjustable shelves. The larger the better if you have the space. I
have gotten mine from garage and tag sales in good condition for between $10
and $40 (they retail for over $200).
Of course, other kinds of cabinets are fine as well. However, anything
you chose should have doors to minimize dust on optical and electronic
components and assemblies.
- Small cabinets with 24 to 50 plastic drawers are most convenient for
electronic, optical, hardware and mechanical parts. One with 50 drawers can
typically be purchased for $10 to $15. I prefer where all the drawers are
the same size - those with multiple size drawers seem just plain silly. :-)
- File cabinets with half-height (index card) drawers and blue print
cabinets are excellent for tools and parts as well. These are unbelievably
expensive if purchased new but sometimes turn up at estate sales and the
like for a song (because most people cannot think of a good use for them!).
- The wall space above your optical or electronics benches can also be
utilized by adding some shelves or even those recycled kitchen cabinets
(which are even better since they have doors!).
I wish I had this! Note:
Two means of exit and two fire extinguishers!
Also note the chair - most important - and the bench for your guest (though
probably should be s eleep-sofa so they can snooze while you spend the afternoon
adjusting your gas mixture or performing mirror alignment. :-)
|<------------------------------- 12' ------------------------------>|
___|____________________________________________________________________|
^ | | | |
| | | Storage Cabinets/Shelves (above work area) | |
| | '---------------------------------------------------------' |
| | Electrical Outlets (two circuits) all along wall |
| | |
| | Work Surface - thick hard-plywood (3' x 12') |
| |____________________________________________________________________|
| | | |
| | | Vacuum System on floor (beneath work area) Gas |
| | | Cylinders |
| | Test | __________|
| | Equip., | ________ | |
| | Power | | | | Wet area |
| Supplies, | | Office | | Glass- |
10'| Misc. | (| Chair |) | working |
| | |________| | Ventila- |
| | | '--------' | tion |
| |___________| |__________|
| | |
| |S Power Switch _ _ __________ |
| |(on Wall) .-======'======-.| | |
| | / | || Bench | \ |
| | / Fire | Storage || | Fire \ |
| | / Ext. | ||==========| Ext. \ |
_v_|__/ _______|_______________|____________________ \__|
- Lab equipment - Scientific supply companies. Surplus outfits.
- Glassware including glass tubing - Scientific supply companies. Some large
hobby shops may have some of this as well but the quality may be poor.
- Gasses - Chemical supply companies, Gas supply companies (e.g., AirCo),
Welders and welding supply companies, neon sign shops and supply companies.
- Chemicals - Chemical supply companies, high school/college teaching or
research labs, your local grocery, pharmacy, hardware store, home-center, and
supermarket! Not all chemicals are exotic and hard to find!
- Electrodes - Neon sign shops, fabricate your own
- Optics - New, surplus, salvage (e.g., broken HeNe laser tube to obtain
dicroic mirrors). Check out the various suppliers listed in the chapter: Laser
and Parts Sources. Note: A basic requirement for going through life should
be at least one trip to to the Edmund Scientific's outlet store!
- Mirror alignment jig. It is a simple matter to make your own. For these
relatively wide bore lasers, this can be done using simple materials (like
cards with holes punched in them, flashlight bulbs, and microscope slides. Or,
if you have an HeNe or collimated diode or other working laser, using that for
a light source. There are at least two alternative basic parts type designs in
"Light and its Uses" and laser based designs in the chapters: Helium-Neon
Lasers and Argon/Krypton
Ion Lasers.
- Structural materials - Scrap/salvage/junk yards, Lumber yards,
Home-centers, Machine/metal shops. Sometimes common household items are
overlooked - be creative.
Develop a relationship with a
teacher/instructor/professor/researcher at a high school/technical
school/college/university/industrial lab. Some people will be more than eager to
help and mentor you - even to the extent of loaning equipment or donating small
quantities of chemicals, electronic components, hard to find optics, etc. to
your cause. Use of their lab may even be possible. There are various programs as
well to encourage students to go into science and technology fields. Who knows,
they may even pay you to do this!
Call up laser and optics manufacturers. Sure, many won't give you the time of
day unless they think you will be ordering $1,000,000 worth of equipment. But,
all you need is one to say yes! There are always such things as cosmetic rejects
or seconds - that are useless to them because they cannot sell the parts - but
fine for your needs. The trick is to hold their attention long enough - or be
such a (polite) pain in the neck that the easy way out is for the company to
provide what you want! I have heard of people obtaining all sorts of material,
parts, equipment - some of it quite expensive - in this manner.
In summary - possible places to find useful stuff:
- Household items.
- Scientific equipment/chemical supply houses
- High school/college/university labs
- Industry, particularly laser, optics, and scientifically oriented
companies.
- Metal, wood, and plastic fabricators, neon sign shops.
- Garage sales, flea markets, hamfests, thrift stores, etc.
- Hardware stores, home centers, pharmacies, variety stores, supermarkets.
(From: Chris Chagaris (pyro@grolen.com)).
Here are a couple of resources that I have not seen mentioned anywhere on the
Net:
For chemicals used in various aspects of laser construction and laboratory
glassware at unbeatable prices, a fine source is:
- Hagenow Laboratories Inc.
1302 Washington Street
Manitowoc, Wis.
54220
Phone: 1-920-683-3339
This company has been in business since 1953 and does welcome orders from
individuals. Some of the materials that may be of interest to the laser
constructor are: Methyl and ethyl alcohols for dye laser solvents, copper
chloride for the CuCl2 laser, mercury metal for vacuum work ($7.25/4 oz.!),
and West type, glass, condenser tubes with water jackets up to 600 mm in
length, for use as plasma tubes in CO2 laser construction.
For
quartz tubing and quartz windows of all sizes, at very good prices, may I
suggest:
- G. Finkenbeiner Co.
33
Rumford Ave.
Waltham, MA 02154
Phone: 1-781-899-3138
Fax:
1-781-647-4044
Email: GFIglass@aol.com
Web:
http://www.finkenbeiner.com/
I have dealt with them personally and found them to be very receptive and
helpful. They, of course, also do precision glasswork of all kinds and
specialize in working with quartz.
On a side note, they are the only manufacturers in the world of Ben
Franklin's invention..... The glass harmonica!
I would be glad in
assisting other individuals in locating some of the more difficult to procure
items needed in some aspects of constructing these various lasers.
(From: Steve Roberts (osteven@akrobiz.com)).
If you are into building your own HeNe (or other) laser from the ground up,
these suppliers may come in handy.
- Coherent Auburn Group.
- Spectra-Physics, a large-frame HeNe
maker, might be willing to donate/sell at cost. 1-415-966-5576
- Dale Harder of H and H Lasers, Inc., Cleveland, Ohio (sorry, don't have
his current phone number). He rebuilds large HeNe lasers (up to 120 mW) and
knows what you need and probably has old ones.
- Holo Spectra, Inc., phone: 818-994-9755. Contact Bill Arkin.
- Midwest Laser Products, phone: 708-460-9595.
- Meredith Instruments, phone:
602-934-9387.
(From: Joe or JoEllen (joenjo@pacbell.net)).
A good resource for components found in "Light and it's Uses" is:
- North Country Scientific
RFD 1
Plymouth, NH 03264
Phone:
1-603-726-3532
I just spoke to the owner-nice fellow. He says he still has inventory of
some nitrogen, argon, dye, and Hg Vapor laser components but interest is
dwindling so I don't know how much longer he will be in business. His prices
are very good also.
Back to Amateur
Laser Construction Sub-Table of Contents.
Introduction to Vacuum Systems and Technology
This and the sections that follow
represent the barest introduction to vacuum technology and systems. See The Electronic Bell Jar
for additional articles, links, and references on vacuum technology of relevance
to the hobbyist and experimenter. In particular, Vacuum Basics
provides a nice introduction including vacuum terminology and applications.
Its parent site, the
Bell Jar has an index to many additional articles available only in hard
copy and/or by subscription.
There have also been a number of articles on vacuum systems and technology in
the Amateur Scientist column of Scientific American. See the Index to the
Amateur Scientist articles maintained by the Society of Amateur Scientists.
These include:
- Vacuum pump, December, 1958, pg. 134.
- Vacuum pumps, March, 1960, pg. 187.
- Vacuum leak detection, February, 1961 Feb, pg. 159.
- How to make a Valveless pump, January, 1965, pg. 118.
- How to make a McLeod gauge, December, 1965, pg. 106.
All but one
of the gas lasers described in chapter: Home-Built
Laser Types and Information require a decent vacuum system to remove air
from the laser tube so that it can be back-filled with the required lasing
gasses at a low pressure - a vacuum. These include the HeNe, Ar/Kr, CO2, HeHg,
and CuCl/CuBr lasers. The N2 laser requires only a 'low' vacuum since it runs at
a substantial fraction (e.g., perhaps 20%) of atmospheric pressure and some
versions can run ambient pressure (1 atm).
The vacuum system serves three functions:
- Remove (nearly) all the air from the apparatus. For almost all the gas
lasers we will be describing, air is poison. It must be purged from the tube
before the required gasses can be admitted. Only with most of the air gone,
can proper and efficient lasing action to take place. Even a small amount of
residual air may result in erratic or weak operation - or no output beam at
all!
- Pump out residual gasses resulting from outgassing from the glass, seals,
adhesives, finger prints, and other contamination on the surface and in the
crevices of the laser tube assembly. Some materials like vacuum grease do not
cause problems. However, a single finger print can represent a veritable
reservoir of unwanted vaporous contamination!
- Control the pressure of the gas fill as individual gasses or gas mixtures
are admitted to the apparatus either prior to or during operation as the
electrical discharge buries gas molecules under sputtered electrode material
or chemical reactions affect the proportion of each type of gas.
By
the standards of the vacuum industry, our requirements are modest and are not
really termed a 'high' vacuum but they are still not the sort of thing you come
across in daily life.
But first, how about all this talk of pressure?
We always hear about the barometric pressure - or the level of a
vacuum - in terms of 'mm or mercury' or 'inches'. 1 atmosphere (at sea level
under some unidentified ideal conditions) is also said to be 14.7 pounds per
square inch. Why?
The earth is covered with a vast ocean of air. Despite common experiences,
even air has mass and mass implies weight. We know it has volume or else your
automobile would have a real problem with flat tires. Most of the volume (the
contribution from the volume of the the protons, neutrons, and electrons in the
atoms are negligible but not precisely zero) results from the constant motion of
the molecules (in air or other gas) bouncing against each-another due to their
thermal motion. This also keeps the air in a gaseous state. At really low
temperatures, the motion is reduced resulting in liquid and solid phases of even
air. At exactly absolute zero (-459 degree F or -273 degrees C) all motion
ceases. However, even then most of the volume of the frozen air is still empty
space - but that is another story.
At sea level under average conditions, the column (actually an inverted
truncated pyramid if you want to be strictly correct) of air above 1 square inch
of area would weigh 14.7 pounds if you could capture, compress, and package them
and plop them down on a delicatessen scale! As you move away from the earth,
this 'column' of air becomes increasingly rarified approaching a prefect vacuum
at 50 miles or so - else low earth orbit satellites would not stay up very long
due to air friction.
It turns out that a column of mercury with an area of 1 square inch and 29.92
inches (760 mm) high weighs exactly 14.7 pounds as well (what a coincidence,
huh?). So, if you take a closed-end tube a little more than 30 inches long, fill
it with mercury, and invert it in a pool of mercury, the pressure of the
surrounding air will be able to support a column of mercury 30 inches high. The
space above the mercury will be a decent vacuum. You have made a mercury
barometer.
If you were to take this barometer and place it inside a vacuum vessel and
start up the pump, the column would go down until at the point of a perfect
vacuum (not achievable but close), it would be precisely level with the
surrounding pool of mercury.
Note that the diameter of the tube doesn't matter - wider implies a heavier
column of mercury but the area of the air acting on the column changes by the
same factor. In fact, it can have pretty much any convoluted shape you want
(except that if portions are too thin, surface tension becomes a factor) as long
as it is sealed and totally filled with mercury. Why this is so is left as an
exercise for the student!
The corresponding height of 1 atmosphere for water is about 34 feet - a
column of water with a cross sectional area of 1 inch and height of 34 feet
weighs 14.7 pounds. This also means that for a diver, the water pressure
increases by 1 atm for each 34 feet of depth. Thus it is not surprising that
there are significant problems in deep sea diving! You have to go up by MILES in
air for the pressure to decrease by a substantial fraction of 1 atm but need
only go down 34 feet in water to increase pressure by 1 atm!
Note that the most likely form of a pressure you are familiar with is the
reading on the gauge you use when checking or filling your automobile or bicycle
tires. However, this is calibrated relative to the surrounding pressure of
around 1 atm. Thus, the actual pressure inside a tire will actually be 1 atm +
the reading on the gauge. And you thought you had a perfect vacuum inside that
flat tire when the reading was 00.0! :-)
Vacuums come
in all shapes and sizes - and I am not referring to vacuum cleaners! Any local
reduction in air pressure significantly below standard atmospheric pressure (760
mm of mercury, 14.7 pounds per square inch) is termed a vacuum (except by your
local weather person who talks about 'low pressure areas'). For convenience (and
because there must have been a meeting of elder statesman with nothing better to
do), the Torr in honor of some Italian named Torrecelli is used to designate a
pressure of 1 mm of mercury I guess referring to 'Torrecellis' all the time
would be too confusing. :-)
The Vacuum
Chart provides a nice instant summary of pump types, gauges, and
applications, as a function of the level of vacuum.
The following dividing lines between low, medium, high, and ultra-high
vacuums are somewhat arbitrary but will be convenient for discussion:
- Biosphere: 1 atm (760 Torr) to .5 atm. At sea level, the average pressure
is about 1 atm. The weather person will talk about 'inches of mercury' instead
of 'mm of mercury' since most people in the U.S.A. at least haven't entered
the metric age. :-) 29.92 inches = 760 mm. The wildest storm imaginable
doesn't produce variations beyond a few percent of this nominal value.
Mountain climbers have to endure reduced pressure and above about 10,000
feet, require breathing equipment. Anyone who has traveled by air knows the
standard speech at the beginning of each flight "....should oxygen be needed,
the compartments overhead....". This would also happen above about 10,000
feet.
Astronauts on American spacecraft (at least they used to), breath unaided
at a pressure of perhaps 1/5 of an atm because they breath nearly pure oxygen.
Since in the normal atmosphere, oxygen is only about 18 percent of the total
mixture (most of the rest is nitrogen with a little CO2 and inert gasses
thrown in), the resulting biological activity (and the flammability of common
materials, for that matter) is about the same but there is no need to carry
the approximately 80% of useless other gasses and the stesses on the
spacecraft structure (from the difference between the internal pressure and
the vacuum outside) are reduced by 80% as well.
- Low vacuum: 1 atm (760 Torr) to 100 Torr. This is something you may have
dealt with - the suction of a vacuum cleaner, spark advance manifold on your
automobile, a siphon, and so forth. None of these is anywhere near the bottom
end of this range - all are probably better than .5 atm and usually much
closer to 1 atm. All except the smallest incandescent light bulbs are filled
with inert gas at a fraction of an atm as well.
A low vacuum can be obtained by any number of simple mechanical means
including fans and centrifugal blowers, piston and rotary pumps, aspirators,
siphons, chemical combustion and other reactions (which use up the air), etc.
Liquids boil at reduced temperature - often room temperature - in a modest
vacuum but minimal or no precautions are needed to prepare surfaces and
equipment since any outgassing is small compared to the remaining air.
- Medium vacuum: 100 to .1 Torr. This is the range where most of the gas
lasers operate. In addition, neon signs, fluorescent lamps, and other glow
discharge tubes, distillation pumps, vacuum packing, and so forth require
medium vacuums.
A medium vacuum can be achieved with a high quaility mechanical pump.
- High vacuum: .1 to 1E-6 Torr. Crooks radiometer (that thing with the black
and silver vanes that spins in Sunlight), small light bulbs, thermos bottles,
cold cathode (gas type) X-ray and Crooks tubes, mass spectrometers, etc.
At the bottom end of this range true vacuum electronics technology becomes
possible including: vacuum fluorescent display tubes, CRTs, modern hot cathode
X-ray tubes; smaller particle accelerators like cyclotrons and betatrons;
scanning and transmission electron microscopes.
- Ultra-high vacuum: 1E-6 to 1E-14 Torr. The actual vacuum inside the CRT of
your computer monitor or TV is probably at a level of 1E-9 or better. For many
processes, the ultimate quality in terms of yield and performance can directly
tied to the quality of the vacuum used in the manufacturing processes.
To put a 1E-9 Torr vacuum into perspective: If all of the gas molecules
remaining inside a typical 17 inch monitor CRT that had been manufactured at
this level of vacuum were rounded up, captured, and returned to normal
atmospheric pressure, they would occupy a volume of space less than 25 um on a
side - roughly 1/10th the diameter of the dot in the explanation point at the
end of this sentence or half the diameter of a human hair! Yet, inside the
CRT, there would still be approximately 1,000,000,000,000 gas molecules
remaining for unsuspecting electrons to run into!
- Interstellar space: <1E-19 Torr. It is estimated that in the space
between galaxies, there may only be a few molecules per cubic meter - which
isn't much! Think of how much easier it would be to 'fill' CRTs with vacuum
out between the galaxies! Of course, the transportation costs might eat up
your profit margin. :-)
You may also hear the term 'hard vacuum'. I
don't know if there is a precise definition for this either but I would assume
that anything with a low enough pressure to behave similarly to a perfect vacuum
from the normal experiences point of view would qualify.
None of
the gas lasers we will be discussing requires a vacuum better than about .5 Torr
when operating. However, in order to clear them of contaminants in a timely and
economical manner (without a semi-inifinite number of purge and back-fill
cycles), it is desirable to be able to pump down to a much lower pressure than
this. The better your vacuum capability - to a point - the easier it will be to
obtain a pure gas fill. Less gas will be needed (due to fewer pump-down and
back-fill cycles) and time will be saved. However, there is no need to go
overboard. My rule-of-thumb (read: wild guess) is that a vacuum system capable
of reliably pumping down to 1/100th of the lowest operating pressure is adequate
for dealing with a laser tube that has a single vacuum/gas fill port. Pumping to
1/10th the desired final pressure may even be good enough if the laser tube is
fabricated to have a gas-fill port at one end and a vacuum port at the other.
For a flowing gas design (e.g., CO2 laser), the requirements are even less
stringent and just being able to maintain the desired operating pressure may be
good enough. If you think you will be building more than one type of gas laser,
make sure this applies to the one with the lowest operating pressure. Also keep
in mind that some types of lasers (like the HeNe) are particularly sensitive to
the slightest traces of unwanted gasses and a better vacuum system would be
advantageous for these.
Unless have worked with a decent vacuum system in the past, own a HVAC
service business, or just happened to pick up something that looked like a pump
of some kind at a garage sale (but you weren't really sure and got lucky), you
don't have the needed equipment! However, an adequate 'medium' vacuum system can
be put together for less than $400 - possibly a lot less if you are determined
and somewhat resourceful.
Various kinds of vacuum pumps
are needed to pump down to different levels of vacuum. Generally, mechanical
pumps are used for low to medium vacuums and other types are needed to go below
this range. However, there are exceptions.
See Vacuum
Pumps Suitable for Various Home-Built Lasers for diagrams of the types of
vacuum pumps described below that are relevant for our purposes.
There are many types of mechanical pumps but they are usually based on one of
two basic principles: positive displacement (perhaps these should be called
negative displacement in dealing with vacuums!) and turbo-molecular:
- Positive displacement pumps operate on principles that Archemedes would
have understood, sucking in air and expelling it using a piston or rotary
mechanism with valves or vanes of some sort to make sure the working fluid
(i.e., the air or gas in our case) moves in the proper direction. The rotary
type is most common for use with high vacuum systems.
- Turbo-molecular pumps take advantage of the slight but non-zero viscosity
of air molecules. A high speed close-fitting turbine drags gas molecules along
with it around its periphery. You probably won't see one of these high flow
rate pumps turn up at the local hamfest so we won't discuss them further.
These pumps can be further classified as to the number of stages:
- A single stage rotary vacuum pump (sometimes called a 'distillation' or
'disto' pump based on one common application) can achieve a final vacuum of a
Torr or so. This is marginal for some of the lasers we will be discussing but
if one is available, it is worth trying. Also see the section: Salvaged
Refrigeration Compressors as Vacuum Pumps.
- A two (or more) stage rotary vacuum pump is what is generally used for
'roughing' the vacuum - as the initial step in achieving any of the levels of
high vacuums listed above.
A well maintained two-stage rotary mechanical pump (the sort of thing you
find in high school physics departments. OK, perhaps except for the 'well
maintained' part) can achieve a vacuum of 10 milliTorr or less if conditions
are perfect. However, with use, age, oil contamination, and somewhat worn
seals, even 1 Torr may be optimistic. So, if you find one of these at a garage
sale (as I have), it may be necessary to do an overhaul or at least to totally
drain the old oil, flush and drain again, and fill with fresh vacuum oil of
the proper type (available from scientific or refrigeration service supply
houses, not motor oil or 3-in-one!). Replacing the oil may be the single most
important thing to achieve acceptable performance.
Moisture is also a killer of oil, so using such a pump as a wet dry vac
isn't a good idea either!
- High quality small pumps of this type may cost $1000 or more new,
perhaps $500 used.
- An alternative which for light duty use may be just as good for our
purposes is the type of pump used by the refrigeration (HVAC) service
industry. These go for around $350 new and much less used - but may have
been abuse so checking their condition before purchasing is essential.
If you do pick up one of these used, replacing the oil should greatly
improve its performance as all sorts of contamination can be sucked in when
used to evacuate refrigeration systems and there was probably little or no
maintenance ever performed on the pump itself!
The
Electronic Bell Jar has a detailed article on these types of pumps.
- Below 1E-4 to 1E-5 Torr, another type of pump in addition to the
mechanical 'roughing' pump is required. This is placed in-line between the
container you are trying to evacuate and the roughing pump. The most common
type is an oil diffusion pump. (Early diffusion pumps used mercury as the
working fluid but the modern synthetic oils are better and are not poisonous.)
A diffusion pump has no moving parts (at least at the macroscopic level). An
electric heating element in its base boils a small quantity of a special
'diffusion pump oil' inside a sort of tower or percolator structure which has
vents to direct the jets of oil vapor downward toward the higher pressure
region (to the mechanical pump) where it condenses on the cool surfaces of the
pump housing and is recycled. In in the process, air molecules are dragged
along with the oil vapor and then sucked up by the roughing pump. The actual
pressure differential between the top and bottom of the diffusion pump is
miniscule - only a fraction of a Torr - but this is adequate to suck out most
of the remaining air or other gas molecules. However, the diffusion pump
cannot be fired up until the vacuum is down to this level.) The pumping speed
is also quite impressive - once it gets going, the pressure drops rapidly.
Diffusion pumps require cooling of their own. This is usually tap water
through a coil wrapped around their exterior though some use forced air
cooling.
For the cyclotron at my high school (right, how many high schools have atom
smashers - but that is another story), we had an air-cooled glass oil
diffusion pump (probably because no one else wanted it). Somehow, this fragile
glass structure survived all sorts of catastrophies despite being located
under the main vacuum chamber situated between the pole pieces of a magnet
weighing several tons and joined by a clamp type glass and O-ring
seal..........
Though no self respecting high vacuum system would be without at least one
diffusion pump, this is not really essential for most of the gas lasers under
discussion. However, if you come across a small one in good condition at a
decent price, you can never tell when your interests might wonder in
directions where a true high vacuum system would be needed.
While
not generally thought of as pumps, the following perform related functions
helping to rid the system of moisture and other unwanted volatile materials:
- Dryer. A canister of a moisture absorbing chemical in the vacuum line may
be desirable in addition to the cold trap.
- Cold trap. Many of the contaminants we wish to avoid/remove condense or
freeze at relatively high temperatures (well, relatively speaking). If a
portion of the vacuum hose between the last pump in the chain is passed
through a container of dry ice or liquid nitrogen, much of this material will
be 'trapped' and effectively removed from circulation as long as the cold
stuff doesn't evaporate. Large vacuum systems will have a large liquid
nitrogen cooled baffle between the diffusion pump and the vacuum chamber.
In addition to helping to achieve a high vacuum, a dryers and cold
traps may also help to prevent contamination to the oil in the vacuum pumps.
How many refrigerators, window air conditioners, freezers, and
dehumidifiers, have you hauled to the dump or passed up on the curb???? The
compressor in these systems may be pressed into service as a vacuum pump where a
low (and in some cases, medium) vacuum is acceptable. A detailed discussion of
this is provided in the hard copy version of the Bell Jar. (The Electronic
Bell Jar being the subset of these articles that are on-line. Check that
site for contact and subscription info.)
- Based on the ratio of displacements alone (ignoring all other losses), a
pump that can achieve a pressure of P (in atmospheres) when used as a
compressor, can produce a vacuum in Torr of 760/(1 + P). Since a typical
*working* pressure (not even the ultimate possible) for a refrigeration system
is several hundred psi (10s of atm), a vacuum below 100 Torr should be easily
achievable with any of these and some will go down below 1 Torr. Note: The
specifications you find in the little service booklet that came with your
refrigerator may only indicate 1/3 atm (250 Torr) performance. Just ignore
them!
- Refrigeration compressors are piston or single stage rotary pumps. (See Vacuum Pumps
Suitable for Various Home-Built Lasers for diagrams including typical
refrigeration compressors.) Therefore, don't expect to achieve 10E-6 Torr or
even be guaranteed adequate performance to provide the rough vacuum for a
diffusion pump:
- Piston compressors will be limited to several 10s of Torr - which is
adequate only for the N2 and possibly some CO2 lasers. This type is found in
most refrigerators, freezers, dehumidifiers, and some air conditioners.
- Rotary compressors are similar to true single stage vacuum pumps and can
achieve an ultimate vacuum of 1 Torr or better - sufficient for many of the
home-built lasers (and other) medium vacuum applications. Apparently, these
are found mostly in air conditioners and the compressor itself is usually
manufactured by Matsushita. My Emerson Quiet Kool(tm) window units use this
type of compressor - but they aren't broke yet :-(. (I believe there was
also a run of GE rotary compressors used in various model refrigerators.
However, as I recall, they had problems and a recall of sorts. Therefore,
you don't want one of those!)
- One way to tell the two apart is that rotary compressors are tall and
skinny (typically 9 to 12 inches tall and 6 or so inches in diameter)
whereas the piston types are short and squat. The piston variety also go
'clunk' when shaken whereas the rotary type are respectfully quiet. :-)
- First, confirm that the compressor is good. While there is no way to be
sure that it will produce an adequate vacuum without tests, if you have the
choice, select a unit that was working, cooling wise. If the rotor is locked
(blows fuses, cycles on the overload) or if it runs and runs and runs and all
that happens is that parts get warm or hot (including the evaporator coils),
the compressor itself may be faulty. These compressors are all of totally
welded construction and essentially impossible to open for repair or even
inspection! If the refrigerant charge has leaked out (little or no hissing and
no frost forms when the lines are cut) but the compressor still runs, it is
probably still good.
- Use a tubing cutter (NOT a hacksaw) to disconnect the compressor from the
rest of the system. This will prevent metal particles from contaminating the
system. There may be multiple ports to the compressor itself but only two
should need to be cut. Once the integrity of the system is breached, just let
everything sit until the Freon bleeds out before cutting completely through.
Then cap the ends to prevent the entry of dirt and moisture.
WARNING: The escaping Freon will be COLD - enough to cause frostbite. Let
it alone until some time after the hissing stops!
WARNING: While Freon itself is non-flammable, poisonous gasses will result
from contact with an open flame. Do this outside!
It is currently against EPA regulations to release CFCs (e.g, Freon) into
the atmosphere and cutting the the refrigerant lines to remove the compressor
without recovering the Freon is against the law. Therefore, consider having a
HVAC service company purge the Freon for you - it is even possible they will
do this free of charge (as long as you deliver and pick up the appliance)
since the recovered Freon is worth something.
- When ripping things apart, don't forget the starting relay, capacitor (if
any), and thermal protector ('Guardette' in the typical schematic) and make a
note of the wiring. Then, mount it on a solid wooden base the same way it was
oriented in the original appliance and wire it up to its own cord, switch, and
plug! See the sextion: Salvaged
Refrigeration Compressor Wiring
- Since these compressors depend on the cold Freon entering via the suction
line to help cool the internal mechanism, the unit may run hot if operated
continuously. Leaving the thermal protector in the circuit will at least shut
down the system before it gets too hot. A fan blowing on the case may help.
However, since pumping from a perfect vacuum (yeh, sure!) to 1 atm is a lot
less work than compressing to the many atm required normally for
refrigeration, the heating may not be that bad - but operation overnight for
roughing a diffusion pump may be pushing your luck!
- During normal operation, oil circulates with the refrigerant. With the
loop broken (after all you are only sucking!), some types will be starved of
lubrication. Such 'pumps' have been reported to be quite reliable under these
conditions with only an occasional squirt of oil into to the suction line but
I don't know how to predict this based model number or external appearance.
So, your mileage may vary.
It is critical that there always be adequate lubricating oil in the system.
There is no telling how much was actually in the compressor when you cut it
away from the rest of the appliance. An HVAC service company may be able to
help. Some of the proper oil can be SLOWLY added via the suction port (some
compressors will be damaged attempting to compress an incompressible fluid if
it is added too quickly). If too much oil is in the compressor, it will spurt
out the pressure port in excessive quantities.
- Provide a glass wool or similar filter and container on the pressure
port to catch oil that is ejected there to prevent a mess and so you can
keep track of how much is lost. During operation, check the amount of oil in
the container from time to time. There will always be a small amount of oil
expelled out the pressure port. However, if the loss becomes too great, you
will have to add some oil to maintain adequate lubrication.
- In principle, it would be straightforward to implement an automatic oil
bypass system to return expelled oil to the suction port - a simple float
operated needle valve that opens only when the oil level in the output
container exceeds a set value (to prevent air from entering the suction
side). Details are left as an exercise for the student. :-)
In any case, to prevent oil from back-streaming into the vacuum system,
provide a filter in-line with the compressor suction port.
- The metal tubing found in the evaporator and capillary (aluminum or
copper) and condenser (probably steel) of a refrigeration unit may also be
useful but must be cleaned thoroughly of all contaminants like oil if it is to
form part of the vacuum side of your system.
- It may be possible to two such units in series to achieve a better vacuum
but you will just have to try it to be sure!
The
following applies to a typical GE refrigerator compressor. YOURS MAY BE
DIFFERENT! Don't rip out the compressor without making a wiring diagram and
saving all the relevant parts!
The sealed unit has 3 pins usually marked: S (Start), R or M (Run or Main),
and C (Common). The starting relay is usually mounted over these pins in a
clip-on box. The original circuit is likely similar to the following:
|<- Starting Relay ->|<---- Compressor Motor ---->|
___ L
AC H o----o o--------------+--o/ S S
"Guardette" | o---->>-------------+
(Thermal +-+ |
Protector) )|| +-+
Relay Coil )|| )||
)|| )|| Start
+-+ )|| Winding
| )||
| M R/M +-+
+-------->>------+ |
)|| |
Run/Main )|| |
Winding )|| |
)|| |
+-+ |
C | |
AC N o------------------------------>>----+---------+
The Starting Relay engages when power is applied due to the high current
through the Run winding (and thus the relay coil) since the compressor rotor is
stationary. This applies power to the Start winding. Once the compressor comes
up to speed, the current goes down and the Starting Relay drops out.
Note the Thermal Protector (often called a "Guardette" which I presume is a
brand name). Leave this in place - it may save your compressor by shutting it
down if the temperature rises too high due to lack of proper cooling or an
overload (blocked exhaust port or low line voltage).
You can use a heavy duty pushbutton switch in its place if you like or if you
lost the original starting relay :-(.
Two types of valves are required.
Fancy expensive types may not be needed so you may find some of this at your
local hardware store or home center. However, since common valves are designed
to operate in a positive pressure environment, they may not hold up under vacuum
conditions - or they may be fine! In addition, the sealing grease used may
outgas at low pressure. Some testing will be necessary to be sure.
- Shutoff valves are used to isolate a portion of the system or seal in the
vacuum (seal out the air?). For all intents and purposes, all that matters is
that they be vacuum tight and can be opened or closed. Fine control is not
needed.
- Metering valves are used to allow a controlled flow of gas to enter the
system. There are expensive needle valves for this purpose but satisfactory
substitutes can be made by scribing a super-fine groove around the perimeter
of a common conical stop-cock plug.
Some means of determining the precise
level of vacuum is perhaps not totally essential but certainly highly desirable.
Otherwise, whatever you do is like a shot in the dark. The old 'thumb over the
hole' trick really isn't precise enough!
- Direct reading vacuum gauges are based on fundamental principles of gas
compressibility and don't depend on electronic conversion from a a sensor to a
readout. These include Bordon tube, McLeod, and other liquid monometers, and
aneroid (and of course, mercury) barometers.
- Indirect reading vacuum gauges sense some parameter of the remaining gas
such as its thermal conductivity or ion conduction and translate this to a
readout. These include thermocouple and ion gauges.
There are several
types in common use:
- Bourdon tube. This is the sort of gauge you see on air compressors and bad
sci-fi movies - a round body with a pointer and dial operated mechanically.
Basically, the pressure/vacuum is applied to a curved thin walled metal tube.
The amount of pressure differential determines by how much the tube's
curvature changed (positive pressure tends to make it want to straighten out).
The tube's end is attached to a chain and pulley arrangement which operates
the dial pointer. These are adequate for low vacuums and confirming that your
pump is working at all but cannot measure consistently below a few dozen Torr
unless reference (outside the curved tube) is also in a vacuum (which I have
never heard of). The fundamental problem is that the actual atmospheric
pressure (is a storm brewing -> low pressure area?) directly affects the
reading. Since weather conditions can change the local pressure by several
percent (1 percent = 7.6 Torr), it is easy to see why there can be
difficulties with this approach!
- Closed tube manometers. A 'U' shaped tube, sealed at one end, is partially
filled with mercury or other low vapor pressure fluid (like diffusion pump
oil) so that there is no space left above the fluid at the closed end. The
difference in the levels of the fluid in the two arms is an indication of
level of vacuum once it is low enough depending on the difference in height is
accommodated by the size of the tube.
This is essentially identical in concept to a mercury barometer.
By using a valve at the closed end instead of a hard seal, pressure
differences can be measured.
A pair of these is actually adequate for the gas lasers being discussed:
- A coarse gauge using mercury for readings up to perhaps 100 Torr. below.
- A fine gauge using diffusion pump oil for readings from 10 Torr to .1
Torr (though viscosity/surface tension will require a bit of tapping to
minimize error at the lower end of this range.
- McLeod gauge. This is one example of a class of very clever gauges based
only on low tech principles of hydraulics. The second chapter ("More on the
Helium-Neon Laser) in "Light and its Uses" has an extensive discussion on the
construction of a gauge of this type which is quite adequate for our needs.
Unlike the others, this is not automatic - it must be tilted and righted to
read the pressure. This action captures a precise quantity of the rarified
atmosphere which can be balanced against a measured column of mercury.
However, its readings are independent of the type(s) gas in the system
which is advantageous where gas fill is constantly changing.
- Thermocouple gauge. A tube or header has an electric heating element and
thermocouple mounted in close proximity. Since heat conduction is a function
of gas pressure, the temperature of a filament fed with a constant current
will go up as pressure goes down. A thermocouple in contact with the filament
is connected to a meter (possibly via an op-amp circuit) to provide a suitable
readout. Since this is an indirect reading device, it must be calibrated
against a known standard.
Thermocouple gauges operate at the lower end of the range we are interested
in (1 Torr to 1 milliTorr) so if you find a thermocouple gauge *with* the
required sensing unit, grab it.
The article: Building a
Thermocouple Vacuum Gauge includes information on a home-made version
which can be constructed inexpensively.
- Ion gauge. The current which flows at a low voltage between a heated
filament cathode (negative) and anode (positive) is a sensitive function of
gas pressure in the high vacuum range - 1E-3 to 1E-8 and beyond. Protection
must be provided to prevent the filament from being energized if the gas
pressure is too high as it may burn out (if there is oxygen in the mix). Ion
gauges are generally standard equipment for high vacuum systems but are
expensive and not essential for our needs since they don't really work at the
more modest range of vacuum we care about.
The flexible tubing that is used to
interconnect various parts of the vacuum system must satisfy several
requirements:
- It must be vacuum tight. Gas has a way of sneaking through all sorts of
materials under vacuum that may not seem porous under ordinary conditions.
- It must not outgas. Common plastics may continue to release gasses which
were precursors or used in their manufacture - that 'plastic' or new car smell
is evidence of this. A suitable material will have no noticeable odor once
thoroughly cleaned.
- If must not collapse when evacuated - true vacuum hose is thick-walled
and/or reinforced.
When in doubt, test a length (e.g., a meter) by
comparing the lowest pressure achievable with your pump(s) capped by the vacuum
gauge and with the tubing in place. The final pressure should be identical.
Three types
of material are used depending on the particular needs:
- Removable fittings. Joints using ground-glass to metal contact and joints
with metal or glass and rubber O-rings require a high quality vacuum grease to
achieve a leak-proof seal and allow for disassembly in the future. This may
also be desirable for use with vacuum hose connections and rubber stoppers.
The usual choice is a silicone based compound appropriately called 'vacuum
grease'. While common lithium axle grease or Vasiline may work at modest
levels of vacuum, there is no telling what volatile compounds these release to
poison your laser.
- Permanent or semipermanent connections. As with plumbing fixtures, a
material may be required to fill in the fine crevices in threaded or
compression fittings.
When I was involved in vacuum work, the favorite was a compound called 'Red
Glyptal' (Red Glyptal Insulating Varnish is made by General Cement. It is
available in small quantites from electronics distributors like Allied: #
796-3670, GC # 10-9002 for a two ounce bottle, and by the quart or gallon from
chemical/scientific supply houses). This is something like a thick red enamel
paint and makes an excellent seal to most types of materials. Epoxy can also
be used for permanent connections.
For threaded fittings that may need to be disassembled, I see no reason why
that white Teflon plumbing tape won't work just as well for medium vacuums at
least. Vacuum grease may even have a high enough viscosity to prevent it from
being sucked out of the threads in this case.
- Vacuum tight adhesives. Where a permanent connection needs to be made AND
secured, an Epoxy (rigid) or RTV Silicone (flexible) rubber compound may be
used. Note: The type of RTV Silicone compound you want does not smell like
vineger (acetic acid) when curing as this may be corrosive.
TorrSeal is another ultra high vacuum compatible cement. It does not outgas
and is for all practical purposes a nonconductive metal when hard - and that
is very hard. No common solvents will touch it so you better be really really
sure that you want the parts connected if you use TorrSeal as they won't come
apart - ever!
Scientific and vacuum supply companies should carry
all of these and other suitable products. Your needs are quite modest compared
to say, the CRT industry, so there is no need to go overboard with ultra high
vacuum sealers. None of these lasers require anything beyond 10E-3 or 10E-4 Torr
anywhere in the vacuum system so the stuff that is guaranteed to 10E-10 Torr is
probably a bit of overkill (but won't hurt except in terms of cost).
Also see: Fabricating
Air-Tight Seals for one approach to making inexpensive seals that can be
easily opened should a tube need to be regassed.
For our simple vacuum system, leak
testing is usually self evident - there are only a few places where leaks can
develop. There are a number of approaches:
- Where possible, seal off various parts of the system until you locate one
which affects the pressure. This is pretty easy where flexible tubing is used
to connect components.
- Tesla coil. A special hand-held spark generator (actually called an Oudin
coil) may be passed over suspect parts of the apparatus. Its discharge will be
'attracted' to a leak since this represents a path to ground through the
residual gas inside the system.
- Water or oil test. Spray some water (or something else) over suspect
joints as the pump is running. If a slow leak is present, the pressure will
drop while the relatively 'thick' liquid is being sucked through the hole.
- Gas leak detector. Since the presense of trace amounts of some gasses will
change the color of an electrical discharge dramatically, this provides a
means of detecting a leak. A probe emitting a small amount of a tracer gas is
run over the apparatus until the color of a discharge inside the tubing
changes color.
- Helium leak detector. For high vacuum work where budget is no option, this
is for you! A special purpose sensor (actually a mass spectrometer tuned to
the helium atom) is connected to the system. Instead of a color change, the
traces of helium drive a meter or activate an annunciator. Simple, huh?
For gas laser work, a
suitable 'minimalist' vacuum system might consist of:
- Vacuum pump - Well maintained (!!!) two stage rotary mechanical type.
Typical choices are either a laboratory vacuum pump or one designed for the
refrigeration service industry. A small pump is fine as long as it can reach a
vacuum of .1 Torr or better.
- Coarse vacuum gauge - Closed-end manometer (mercury filled). Total tube
height of 150 mm to read 0 to 100 Torr.
A Bordon tube type can be used in a pinch but accuracy will be poor at the
low end of its range.
- Fine vacuum gauge - Closed-end manometer (diffusion pump oil filled).
Total tube height of 150 mm to read 0 to 10 Torr (specific scale factor will
depend on density of the oil compared to the density of mercury). Valves on
the closed end and between the two ends would permit relative pressure
readings between the vacuum system and the laser tube to be made.
Alternatively, a McLeod gauge can be used in place of this manometer. A
McLeod gauge can be more precise but will be more expensive and/or more
difficult to fabricate (and more of a pain to use!)
- Cold trap - A 'U' tube in the vacuum line partially submerged in a slurry
of dry ice and acetone, liquid nitrogen, etc., in a thermos or dewer.
- Gas manifold - A valve or set of valves connecting the vacuum line nearest
the laser tube to the gas supplies.
WARNING: High pressure gas cylinders MUST be fitted with proper regulators
to supply low pressure gas!!! You cannot hook a 2,000 psi gas cylinder
directly to your laser!
- Laser tube coupling - Connects the vacuum system to the laser tube (what a
concept!). Appropriate valves must be provided to permit the laser tube to be
disconnected from the vacuum system if desired.
If a diffusion pump is added (between the mechanical/roughing pump and the
dryer), a thermocouple and/or ion gauge will also be needed.
Also
see: A Simple
Medium Vacuum System for some additional ideas on a low cost approach to a
setup that may be adequate for laser construction.
To a
large extent, the life expectancy of a HeNe or other low pressure gas laser will
be heavily dependent on the cleanliness of the interior of the tube and all its
constituent parts and the purity of the final gas fill. Therefore, while it may
be possible to use a marginal vacuum system and less than super pure gasses with
common basement workshop conditions to get a home-built laser to work for a
short time, don't expect optimum output power or stability and a useful lifetime
for such a tube if sealed off to be more than a few dozen hours, if that!
The following comments come from someone who has experience with both HeNe
and ion laser refurbishing:
Letting a HeNe laser tube up to air outside of a inert gas glove box is not a
good idea. A class 1000 or better clean room environment with HEPA filtered
inert gas is really needed.
- The getters will form a nice fine powder that can't be removed. This will
interact with the plasma. What you will get is a plasma cannon that shoots a
stream of plasma seeded with barium oxide or a titanium compound right at the
mirrors. I have watched a dusty tube with a plasma jet etch a Brewster window
from the back side in a ion laser, that tube was shot in just a few minutes.
- The dust on the optics from a normal room environment kills lasing
entirely or results in chaotic low power lasing. These particles result in a
very unstable plasma.
- The gasses must be pure. That means you have to have extremely dry gas
with no oxygen or water vapor or CO2 or other organics. Water vapor is
extremely hard to pump, and kills lasing like there is no tomorrow. A
mechanical pump will never get rid of it, and getters can barely keep up with
it. Odds are any thing less then a modern high vacuum epoxy won't handle the
bake-out required either. One wonders if it will even cure in a dry inert
atmosphere.
- The fill gas for short lasers must be isotopic, a small lecture bottle of
the proper isotopes is currently at least $800 with a proper regulator. Not to
mention that most modern gas bottle regulators will "run away" full open when
exposed to a vacuum. Both of mine do. Not using isotopic gasses in a HeNe
laser will result in at least a 30% power loss. This, coupled with the poor
vacuum facilities of the average amateur, means that any resulting laser tube
would be just a experiment, not something you could seal off and use.
- 10E-2 Torr isn't enough vacuum. You'll find yourself replacing windows
frequently, or have a sputtering HeNe laser that will only last 10 to 20 hours
if sealed off. What is needed is 10E-6 or better, and that should be the
measured gauge pressure, not the rating on the side of the pump! A cold trap
and a cryo trap are a must. A thermocouple gauge is only around $300 for a
rebuilt one with a decent tube from many vacuum suppliers, without it you are
blind.
- And for those of you ion laser fans using Kovar, lead, silver, tin, brass,
iron, or aluminum in your vacuum system or as part of a tube will probably
result in a poisoned cathode and short life if the plasma or hot gas can touch
it. Note that eliminates most available solders and many brazes; indium-gold
is one of the few brazes that will work.
The main things that
determine your power are, correct Brewster window angle and material (for
external mirror tubes), ultra clean optics, and clean gas fill. We're talking
cleaner then cleanroom clean - better than the best surgical suite -
semiconductor manufacturing type clean!
Back to Amateur
Laser Construction Sub-Table of Contents
Introduction to Glass Working
The following mainly applies
to the traditional gas lasers like the HeNe, Ar/Kr ion, and HeHg where the
entire laser discharge tube is generally a single glass structure - it is made
in one piece from various individual pieces that are fused together. The N2 and
CO2 lasers do not require glass working of this type.
As laboratory apparatus goes, what you need for any of these lasers is pretty
mundane: A few tubes joined together with butt or tee joints, a few dimples or
bumps, some angled cuts, and pieces attached with glue.
Note that at least in principle, it is possible to construct these lasers
without actually fusing glass pieces together as Epoxy or other adhesive and/or
vacuum rated flexible tubes and clamps can be used. However, such a structure is
not nearly as stable and are not recommended. In addition, the added nooks and
crannies of clamped pieces and places with glue that can outgas mean that
achieving the required level of vacuum and maintaining it is much more
difficult.
There are basically two ways to go about obtaining the needed assembly of
tubes, electrodes, Brewster windows, and so forth.
- Have someone else do it! Assuming you can find a cooperative individual or
pay a neon sign shop or laboratory equipment fabricator, this is by far the
easiest especially if you have to start from ground-zero. For someone at all
experienced in this sort of stuff, the assembly of the main portion of a
typical laser tube (not including the Brewster windows) is a 20 minute job if
all the bits and pieces are available. If you can arrange that your design
uses the same sizes and types of glass tubing that they commonly deal with, so
much the better.
- Learn enough of the skill of glass working to do it yourself. This is by
far more fun and who knows, maybe you have a talent for the sort of glass art
exhibited in museums. This really isn't as difficult as it might seem at
first. Glass working is a skill and you will no doubt create some pretty
interesting failures at first. But with a little practice (OK, maybe a lot of
practice!), butt and tee joints, and dimples and bumps will become second
nature. We aren't talking about fancy decorative glass blowing, mostly just
basic cutting and joining.
Glass working as it relates to laboratory
apparatus fabrication has been covered in the Amateur Scientist columns as well.
See: Glass blowing, technique explained, Scientific American, May, 1964, pg.
129.
In the following sections, we provide the briefest of introductions to the
glass working skills that are needed.
What was call glass is made from
silicon dioxide (SiO2) and other additives to produce the wide range of
properties of various glasses that we are familiar: from window glass to Pyrex
cooking and labware; colored glass bottles and stained glass windows, light
bulbs of all shapes and sizes; and optical glass for lenses, mirrors, and
prisms. SiO2 is the same stuff that constitutes beach sand and the insulating
layers of integrated circuit chips.
Glass is an amorphous material - it has no crystalline structure and is
really a liquid at room temperature. A liquid, you say???? Well, a slow moving
liquid at least. As its temperature is increased, glass becomes softer but has
no distinct melting point (compared to water, salt, or any other material that
forms a crystalline structure where there is a distinct phase transition from a
solid to liquid state).
The two types glass which will be of most interest for laser construction
are:
- Soda-lime (S-L) glass is the most widely manufactured type (roughly 90% by
weight) used for plate glass windows, bottles, light bulbs, glassware, a
zillion other common products. It is fairly soft to begin with and can be
worked at a relatively low temperature. S-L glass consists of about 72% sand
or silica, 15% sodium oxide or soda, 9% calcium oxide or lime, and 4% of other
minor ingredients.
S-L glass is not suitable for high temperature apparatus (e.g., the bore of
a high power laser) but should be fine for most other uses.
- Boro-silicate (B-S) glass (commonly called Pyrex which is one brand name)
is much harder and resistant to high temperatures but must be worked at a much
higher temperature as well (a torch burning natural gas and pure oxygne, for
example. It consists of about 80% silica, 4% alkali, 2% alumina, and nearly
13% boric oxide.
B-S glass can probably be used everywhere but the difficulties in working
make this unattactive. However, if someone else is doing the glass-work...
Fused silica (Vycor) and pure quartz are two highly heat resistant
materials that you hopefully won't have to shape since they have even higher
softening (or in the case of quartz, a crystal, melting) points as well!
If you order common laboratory glass tubing, it will likely be made of S-L
glass though other types are also available - make sure you specify what you
want since for some of the laser parts, heat resistance is an issue. Most
beakers, flasks, and anything else that may be heated are made of Pyrex or the
equivalent B-S formulation of another manufacturer. However much other labware
is of the S-L variety. Since the coefficient of thermal expansion also differs
for the two types of glass, there may be problems in attempting to mix them in a
given structure.
For small tubes - say less tha
1/2" in diameter, cutting is, well, a snap!
All you need is a small triangular file (new or in excellent condition, not
rusty and clogged with something disgusting) and perhaps some spit. :-)
- Place the tube to be cut on a solid surface and go over it once at the
desired location with the file - pressing firmly but not so hard that you risk
cracking it right then and there. There is no need to go around the tube - one
location should suffice. The objective is to simply nick the tubing. You don't
need - or want - to be sawing it with the file!
- While holding the tube in two hands, apply a bending force to the tube
with the filed nick away from you - to spread it apart in that direction. It
should snap in two quite cleanly. Once you get the hang of this, the result
will be clean and at right-angles to the tube axis, barely distinguishable
from a diamond sawed cut!
Sometimes, wetting the filed location with a
bit of spit or tap water will aid in the process.
Practice on some scrap pieces of tubing. In on time you will be turning all
the neon tubing in your neighborhood to small bits suitable for making beaded
necklaces!
This also works for larger diameter tubing (like CRT necks) but a longer
crevice may be needed - try to keep it straight. In some cases, one pass all the
way around will be needed.
There are also hot wire cutters (the heated wire produces local stress which
fractures the glass). For large or irregularly shaped objects, the best tool is
a power driven diamond grit glass cutting wet wheel - a water cooled miter saw
for glass and ceramics!
Any sharp edges left by the cutting operation should be smoothed with fine
sandpaper or in the flame of your glass working torch.
All glass working consists of four
steps:
- Heating. This is going to be done with a flame of some kind:
- A common propane torch or natural gas burner using air is just hot
enough to soften S-L glass. A bunsen burner works - barely. Other types of
lab burners are better.
- With the use of pure oxygen, the flames from these all run much hotter
and that is what you is really needed to be able to do any sort of glass
work easily and consistently (or borosillicate glass at all).
- An oxy-acetylene or oxy-hydrogen torch will be needed to easily deal
with some types of heat resistant glass and fused quartz. (CAUTION: Hydrogen
flames tend to be invisible!)
At the proper temperature, glass has the consistency of soft taffy - easy
to bend and shape but not so soft that it runs or drips. Part of the skill
(and fun) is keeping the glass at just the right temperature as it is worked.
As the glass approaches the proper temperature, the flame will take on a
yellow tinge from the sodium ions in the glass (the soda part) and the glass
itself may appear red or orange-hot itself.
- Working: Bending, joining, pulling, dimpling, blowing, etc. is done while
the glass is maintained at a relatively constant temperature in the flame.
Glass cools quickly so repeated or constant heating is needed. Some positive
pressure in the glass parts may be needed to prevent them from collapsing - or
to blow bubbles! The surface tension of the soft glass is going to be both our
friend (since it will help smooth out much of the damage you will inflict) and
foe (since it will tend to want to cause tube ends to collapse or other holes
to expand). Usually two hands and a mouth (safely at the end of a length of
rubber tubing!) are enough but at times you might wish to be an octopus!
- Once the particular joint or whatever is formed to your satisfaction, the
piece must be cooled so that it solidifies. However, you cannot just dunk the
whole affair in a bucket of water as the sudden temperature change will cause
your hard work to shatter into a million pieces (sometimes it will do this
even without such help!) It must go through a process of annealing where a
lower temperature flame is run back and forth over a large area of the glass -
beyond that which was dealt with originally. The cooler flame can be obtained
by reducing the air or oxygen supply to the torch. Fortunately, this takes
only a couple of minutes for anything we are interested in constructing
(unlike the 17 foot diameter Palomar telescope mirror which required over a
year of annealing). Note that there is no real way of knowing how much
annealing is enough - it is just something that one does based on
recommendation or experience.
- Cooling. The worked and annealed area will still be very hot. Set it down
on a non-flammable material or better yet, in such a way that the hot parts do
not touch anything until it is cool enough to touch. This allows it to cool
slowly and uniformaly, further minimizing the chances of stress cracks.
A gas flame (natural gas, propane, etc.)
adjusted for hottest temperature (optimum fuel:air ratio) is divided into
several parts:
Tip---> /\ (Dark Blue)
/ \
Cone --> / /\ \ (Light Blue)
| | | |
_|_|__|_|_
Burner | |
Great diagram, huh?
Note that it is mostly shades of blue - there should be minimal yellow or
orange (indicating that there is adequate air/oxygen) but the flame should not
begin to separate from the burner (indicating too much). There should be no
smoke or soot from such a flame.
The hottest location is just above the inner cone.
With soda-lime glass, once the glass is hot enough to work, the flame will
take on a yellow color due to the sodium ions in the glass.
With the air/oxygen supply cut off, the flame will be long and yellow and may
produce black smoke and soot. This will be the proper temperature for the
annealing step.
Note: Where you have control of the air/oxygen supply as with a professional
glass working torch (or Oxy-Acetyline welder, for that matter), light it up by
first opening just the gas supply a small amount and then adding air/oxygen and
adjusting gas flow after the flame is lit. Shut down in the reverse sequence.
This avoids unsightly pops, bangs, and other explosive behavior.
The only way to really be
come proficient at this is to practice. You will create many many interesting
disasters at first but glass is cheap. After a while, these sorts of 'simple'
procedures will become automatic and second nature. Who knows, even your
failures may find a place in the Museum of Modern Art!
- Smoothing a piece of cut glass tubing:
- Heat the cut end in the flame near the inner cone.
- Watch the edges. As the glass softens, the sharp edges will start to
round off. Even chips and unsightly blemishes will melt away....
- Don't push your luck. If you leave in the hot part of the flame too
long, the tube will close up and you will have to start over (or have fun
and blow a bubble)!
- Anneal for a minute or so and allow it to cool.
- Bending a glass tube.
- Holding the tube at both ends, heat the area of the bend until the color
of the flame becomes yellowish. Keep it moving - back and forth and
rotating. Don't restrict the heated area too much - you don't want the bend
to be too sharp (too localized). A good size to aim for is a bend radius of
no less than 5 times the diameter of the tubing - at least until you get the
hang of all of this.
For large diameter (e.g., greater than 1/4") or thin walled tubing, cap
one end and attach a rubber hose to the other to use as a blow-pipe so you
can apply a little positive pressure (by *gently* blowing into the hose) to
keep the glass from collapsing - don't blow too hard or you will blow a
bubble or rupture the tube entirely!
- Once it is soft, genatly help it along to the desired shape. Don't rush.
When the glass is the consistency of soft taffy, the bend will practically
happen on its own.
- Anneal for a minute or so and allow it to cool.
- Making a butt joint.
- Making a T-joint.
I actually prefer to cheat: Instead of joing a straight piece to the side
of another, where possible, I start with a small glass T connection, cut off
its ends if necessary, and joint it to the main tube using the butt joint.
Depending on the specific diameters and types of glass, this may be a better
approach.
- Flaring the end of a glass tube.
- Cap all but the end to be flared and another one where you attach your
blow-hose.
- Heat the end to be flared until it totally collapses and seals itself.
- Blow into the assembly to create a bubble.
- Continue heating the thin-walled bubble until it melts and then heat the
remaining walls until they flow to the required size.
- Anneal for a minute or so and allow it to cool.
- Creating a dimple.
- Heat the tubing in the precise area where you want the dimple - as small
an area as possible using the tip of the inner cone of the flame.
- Use a pointed carbon rod (which won't stick to glass) to gently indent
the area.
- Anneal for a minute or so and allow it to cool.
Back to Amateur
Laser Construction Sub-Table of Contents .
The Laser Assembly and Optics
The stability and
strength of the baseplate are probably the single most important factors in
determining how easy it will be to set up and maintain a laser with an external
resonator. Multiple optical components have to remain aligned to a small
fraction of a degree despite changes in temperature and placement (on another
surface like a lumpy tabletop) of the laser assembly.
Forget about most wood - it is too flexible, absorbs moisture and warps or at
least changes size all too readily. It may be possible to totally seal some high
quality wood or wood-based composite products but it probably isn't worth the
effort.
Start with a solid metal base. Short of something milled from a big heavy
casting or the use of a real optical bench or table or a converted lathe bed,
the best is an extruded aluminum box shape since this is very strong for its
weight and will resist bending and twisting. A C-channel extrusion will be
nearly as good if it is braced at multiple points along its open side - and this
is more accessible for attaching screws and whatever from underneath. Or, a thin
removable cover plate can be screwed to the open side.
Buying a big enough piece of this new - say 4" x 2" x 4 feet, more or less
depending on the size of your laser - will set you back a few bucks but will
save a lot of time in the long run.
Drill and tap holes for mounting the laser tube, mirror mounts, and whatever
else you need. With tapped holes, there is less opportunity to spend your time
fishing for lost screws! Add keying holes for assemblies that may need to be
removed and replaced without changing their position - like the mirror mounts.
Attach some non-slip material on the bottom to force the entire affair to stay
put!
There are several considerations
when selecting a material to be used for a Brewster or other window through
which light must pass undisturbed:
- Optical quality. This refers to the surfaces (plane, flat, and polish) and
purity of the material.
High quality microscope slides (not the kind that are 100 for $1.00 at your
local hobby store) are actually quite good. To check, hold one at arm's length
and view a distant scene through it - there should be no detectable distortion
or shift of the image as it is inserted/removed from the view. Alternatively,
insert/remove the slide from the path of a laser beam projected onto a far
wall (reflecting back from a mirror to a nearby screen if you don't have a
partner). There should be no noticeable shift in the position of the projected
spot with/without the slide in the beam.
- Index of refraction (and dispersion if multiple wavelengths are involved).
This will mostly affect the Brewster angle, percent reflectance with respect
to window angle, and angle of total internal reflection.
- Heat absorption/losses. This can be critical where the window is part of a
low gain laser resonator as in the case of the Brewster window for the HeNe
laser. Quartz should be better than common glass in this regard.
Keep in mind that the light intensity *inside* the resonator is going to be
many many times greater than the actual power in the output beam. This ratio
will be approximately 1/(1-Roc) where Roc is the reflectivity of the Output
Coupler (mirror reflectivity specified between 0 and 1).
For example, with a HeNe laser, a typical Roc is .99. So, the power level
between the mirrors will be roughly 100 times greater than the actual power in
the output beam - or 1 WATT for a 10 mW laser!
Thus, absorption->heat losses can be significant and need to be
minimized. (And no, you cannot stick a mirror in at an angle to extract a high
power beam but think about zig-zag paths through laser gain media if you have
trouble sleeping some night!)
See the section: Sources
of Supplies for low cost suppliers of high quality optical windows.
The equation for the
Brewster angle defined between the window and a plane perpendicular to the
direction of the light rays (tube axis) is: Brewster angle = arctan(index of refraction)
For a quartz window - desirable for an HeNe laser due its lower heat
losses at 632.8 nm, the index of refraction is 1.54 resulting in a Brewster
angle of 57 degrees.
So, this is a piece of cake even if you weren't a stellar performer in high
school trig. However, suppose you don't know the index of refraction of the
material you are using? Ah, no problem if you have a light source (like a laser)
of the SAME wavelength since it can be determined experimentally. For the
construction of the HeNe laser this should be no problem since you likely
already have some sort of HeNe laser! And, we already warned you that you
shouldn't be building the HeNe laser if your goal is just to have a working HeNe
laser anyhow. :-)
The light source has to be polarized. This either means a laser outputting a
polarized beam (by design or see the section: Unrandomizing
the Polarization of a Randomly Polarized HeNe Tube) or the use of a
polarizing filter on its output. However, for the latter, common HeNe tubes
produce a beam with random polarization - it varies as the tube heats up and
just because it feels like it! This means that the intensity will be varying at
the output of the polarizer so this will have to be taken into account as you
view the reflected beam.
- Fasten a sample of your window material to a block of something so it is
perfectly vertical and in a way so that it can be adjusted between about 30
and 70 degrees with respect to the direction of the laser beam and that the
angle can be accurately measured.
- Line everything up with the window at a 45 degree angle and turn on your
laser.
- Rotate the laser or its polarizer about the axis of the beam until the
reflection off the window is minimized (keeping in mind that your actual beam
intensity may be varying at the same time if you have a random polarized HeNe
tube).
- Adjust the angle of the window until the reflection is further minimized.
Repeat steps 3 and 4 until the reflection is as small as possible.
When optimal, the reflection should be extremely faint. Measure the angle. :-)
When most people think of mirrors, what they
use for shaving or makeup or the rear or side view mirrors of the automobile
come to mind. However, none of these would be permitted anywhere near a laser
lab. To put it bluntly, their quality and performance stinks!
The ideal mirror would have a coefficient of reflectivity of 1 (100%) for all
wavelengths of interest and produce no distortion.
- Optical quality mirrors are usually 'front surface' coated which means
that the reflective layer is on the front of the supporting structure rather
than behind as in the case of a common household glass mirror. Otherwise,
there will be a ghost reflection from the front (uncoated) surface and
degradation from passage through the mirror material (glass, plastic, etc.)
- For many applications, metal coated mirrors are fine. Aluminum and gold
are common (well, ok, maybe not so common for gold) materials that have decent
reflectivity at a wide range of wavelengths. However, even the best metal
coating has a reflection coefficient of less than .99. This may not matter
viewing your face in the morning or even for bouncing a laser beam around an
optical apparatus. But where every last fraction of a percent counts, another
type of mirror coating is needed.
- Where performance is critical, the mirrors are not silvered or aluminized
(metal coated) but are a type called 'dichroic'. They are made by depositing
many alternating layers of hard but transparent materials having different
indexes of refraction. The thickness of each is precisely 1/2 the wavelength
of the light for which the mirror is being designed. This results in
reflection by interference with very high (>99.9 %) efficiency - much
greater than for even the best metal coated mirrors. On either side of the
nominal wavelength, reflectivity falls off so this type of mirror may not a
useful without additional work where a wide range of wavelengths is involved.
Mirrors are used in two sorts of places: as part of the resonator and
everywhere else.
- Mirrors which are part of the resonator are special in that they affect
the performance of the laser directly. Percent reflectivity with respect to
wavelength, surface figure and finish (shape as in planar or concave and
quality) are all critical.
- Dichroic (interference) types are almost always used.
- Planar or concave mirrors may be used at each end. Where a concave
mirror is used, its radius of curvature is usually about equal to the
distance between the mirrors. This is called a 'confocal' arrangement and
results in somewhat easier adjustment of the mirror alignment - it is
somewhat forgiving. However, planar mirrors result in higher efficiency
since more of the lasing medium can participate (think of the shape of the
reflected beam inside the tube).
Needless to say, you aren't
going to find resonator-qualified mirrors at the local variety store! Unlike
aluminized telescope mirrors which are possible to coat in your basement (at
least in principle), this is not an option for dicroic types. They can be
obtained from optical supply companies and in the case of the HeNe laser, dead
or sacrificial HeNe tubes. (Argon or krypton ion also, but you aren't likely to
have any!)
The HeNe, Ar/Kr ion, HeHg,
and other similar gas lasers all require adjustable mirrors outside and usually
separate from the tube itself. These should be:
- Solid, rigid, and stable with respect to temperature and humidity.
- Easy and intuitive to make fine adjustments.
- Easy to remove and reinstall with minimal effect on setting (as when doing
initial alignment, for example).
- Inexpensive and easy to fabricate. :-)
You can of course purchase
such mounts but one of them will probably set you back more than the entire
budget for this laser project! However, there are homemade alternatives.
The Adjustable Mirror
Mount is a simple design that meets all of these requirements. It consists
of a right angle aluminum bracket, an aluminum plate to which the mirror is
attached with glue (around the edge), screws, or clips, and three spring loaded
thumb-screw adjusters. Indexing balls between the base and the mounting surface
and an adjustment screw allow it to be removed and replaced with virtually no
change in alignment. These can be constructed using common hand tools though a
drill-press would be nice and high quality drill bits and taps are a must!
Parts list (typical):
- 1 - Aluminum L-bracket: 2.25" L x 3 W x 3.5" H, .125" or thicker.
- 1 - Aluminum plate: 3.5" diameter (trimmed, if desired), .062" or thicker.
- 4 - Thumbscrews: 10-32 x 3/4". Finer threads are even better.
- 3 - Compression springs.
- 3 - Flat washers: #10 x 1/2" outside diameter.
- 3 - Steel or glass balls, 1/8" to 1/4" diameter.
A similar design
may be found in "Light and its Uses".
Basically, the procedure below is a means of using the optic
(mirror) to image a source at infinity thus providing the focal length and, from
this, the radius since for a mirror, r=2f.
(From: Steve Roberts (osteven@akrobiz.com)).
Take a working HeNe laser, upcollimate it to at least 10X the size of its
normal beam, and make sure it has 1/10 the normal divergence, in other words
just expanding it with a lens wont work, it must have all the rays in it
parallel. Or, take a large diameter source of projected light focused at
infinity, and aim it at a slight angle from the normal to the optic. (Normal
means at exactly right angles to the surface.) The optic should be many feet
away from the light source. Then you should have the beam coming back toward the
source but not hitting it. If it's a flat or convex mirror, the beam will
continue to expand. But, if it was figured with a concave radius during
polishing, by sweeping a card through the reflected beam you can sometimes find
a focal point. Measure the distance from the focal point to the surface of the
optic, this is 1/2 of the radius so double the measurement to get the radius.
This isn't that accurate, but it will give a measurement within 10 percent. You
are probably never going to find a convex ion or HeNe optic, but you might find
them in CO2 or YAG lasers.
For ion laser optics, standard radii are flat, then 60, 100, 200, 300, 400,
800 cm. Generally the optic focal length is at least twice the length of the
plasma tube if the rear mirror is flat, for a TEM00 beam.
The following is from someone who is involved in commercial laser
repair and even he has problems finding suitable low cost replacement optics!
I recently went hunting for laser optics. A pair of standard coated 12.5 mm
diameter mirrors for an ion or HeNe laser would set you back $1200-2000 a set,
you might get a suitable rear mirror for a Hg, CuBr, or CO2 for much less, but
the price of optics for any gas laser will be prohibitive. Large frame argon
laser optics, if you could find a used set, are going to be $250 for optics if
the coatings are still anywhere near useful, and much more if they are in good
shape. Costs seem to stay the same regardless of the substrate material or
diameter - buying a smaller optic won't be that much less expensive if at all.
If you are thinking about going direct to a supplier of laser optics, off the
shelf optics similar to what they coat for other laser companies are generally
not available as the contract prohibits the optics company from selling them.
Thus yours will be a 1 off custom run. The low cost Chinese optics companies do
not do ion or HeNe coatings with the needed levels of reflectivity or quality. I
tried that too, and I have especially good relations with one of them.
You have to rip them out of a dead laser of similar size and power, and for
HeNe this is a problem as modern sealed HeNe tubes may use at least one mirror
that is concave and is only good at the same working distance between the
mirrors used in that given tube.
I know, I just spent two months hunting down an ion set, $750$ a optic new,
so $1500 for a full cavity for a 1 meter class laser. That was a relatively
inexpensive optics set too. It was for krypton or I could have bought a whole
used 1.7 W argon ion laser for not much more.
Using the short radius semiconfocal cavity optics of an ALC-60X or Omni-532
for the Scientific American tube will not work even though the mirrors are only
$300 a set for cheapies. Mirrors are coated to a specific transmission based on
tube length, a small air cooled might be .6 percent transmission, where a 2
meter long large frame 25 to 30 watt would be around 8%, but that percentage
would be tailered across the range of lasing wavelengths for a specific balance.
So if you tried using a 2 watt pair of optics for a 10 mW homemade laser, you
would be very sadly disappointed in the output and/or it probably wont lase at
all, or if it did you would only see the ultra high gain 488 line lasing.
However mirrors for a shorter low power laser might work if you scale up the
tube. The problem will be the radius of the mirrors, not the transmission. For
example, a 1 meter radius ALC-60X OC might work for Scientific American ion
laser, but the usual standard 60 cm radius would not. Plus aligning a non
optimized cavity would be a bear, and with a low gain amateur tube, highly
unlikely. Funny how the author left the optics specs out entirely!!!!
For a recent project we put two 45 cm radius optics from a laser with a 1.5
inch longer resonator then a 60X into a 60X, alignment time approached 1 hour
instead of the usual 5 minutes, and did not get any quicker. There was exactly
one path with respect to the bore that worked, including the offsets in length
caused by the X-Y adjustment screws on the end plates, talk about critical!!
Only reason we did it was we needed gain on a line not supported by the 60X
optics for a experiment.
So what I'm trying to say, is, unless you have the right optics, you are
better off investing in a working laser if you are trying HeNe, or Ar or Kr ion.
There are only 3 companies in the US who produce hene mirrors, and the one of
them that was hobbyist friendly just told me, "no more" as they are tired of
coating optics that get returned with the claim "well my tube is good, so it
must be your mirrors that aren't working, or for argon, I don't like the
green-blue-red balance or transmission of these optics."
Back to Amateur
Laser Construction Sub-Table of Contents
Power Supply Considerations for Home-Built Lasers
Also see the section: Related
Power Supply Information for much more on high voltage and other specialized
power supply operating principles, design, components, and construction
techniques.
Several types of power supplies are used for these lasers (more than one type
may actually be applicable).
- AC. A high voltage transformer supplies an alternating voltage (at the
power line frequency - 50 or 60 Hz) to a pair of electrodes roughly at each
end of the laser tube. The amount of voltage/current/power is usually
controlled by using a Variac (variable autotransformer) to power the system.
There are usually no other components beyond possibly a ballast (series
current limiting) resistor.
Luminous tube (neon sign) and oil burner ignition transformers are the most
common types, are simple to use, and relatively easy and inexpensive to
obtain. These typically produce between 5 and 15 KV at 10 to 60 mA and are
internally current limited. (The implementation uses a loose magnetic coupling
but the effect is that of a series resistor that limits current to the maximum
specification when the output is shorted).
Check demolition companies, salvage yards, neon sign shops, etc. They sell
old transformers at low prices since a guarantee for long term reliability
cannot be provided - but you really don't care unless your laser is to be run
for years on end. Oil burner types will be totally free from HVAC contractors
- but you will probably have to take the entire smelly, oily, icky oil burner
away as well!
- DC. The output of a high voltage transformer or high frequency inverter is
applied between a pair of electrodes roughly at each end of the laser tube.
Current through the tube may be controlled by adjusting a Variac as above
and/or by providing an appropriate ballast resistor (as with a conventional
HeNe laser power supply - see the chapter: HeNe
Laser Power Supplies).
The output of luminous tube and oil burner ignition transformers can be
rectified and used to charge high voltage capacitors. However, both the
rectifiers and capacitors must be rated for the voltages involved.
- Pulse. A DC power supply charges up an energy storage capacitor which
either discharges between electrodes in the laser tube (or flash tube) when
its voltage rises high enough, when the pressure goes (is pumped) low enough,
or when the gas in the tube is ionized by an external trigger generator like
that of a common electronic (xenon) flash.
Timing may also be provided by mechanical means - a rotating switch or
commutator arrangement feeding the outputs of multiple high voltage capacitors
to the laser tube in sequence like an automobile engine distributor.
High frequency inverters may also be used as the power source for
any of these approaches.
- RF. Electrodes or coils outside the laser tube are excited by what is
essentially a radio transmitter power oscillator. Although the first HeNe
laser used this approach, RF excitation doesn't produce a high enough
intensity of the discharge where it is needed - in the center of the tube bore
so it is usually not appropriate.
It is unlikely that you
will have or can find exactly the types of meter needed for each of these
lasers. However, any sort of mA or uA meter cn be turned into a DC or AC voltage
or current meter of almost any full range sensitivity quite easily. This can be
a moving coil (D'Arsonval) type or digital panel meter module. For historical
reasons, we call these 'movements' whether they have moving parts or not. :-)
In the discussion below, Im is the full scale sensitivity of the meter
movement and Rm is the resistance of the meter movement.
- For the voltmeters, the series resistance has been divided into a fixed
(R1, R3) and variable (R2) for easy calibration. There are some special
requirements for high voltage voltmeters in particular:
- Try to select R1 versus R3 taking into account which end, if any, of the
circuit is at ground potential to place the meter itself and the calibration
pot (R2) near ground potential as well.
For centertapped HV transformers (e.g., luminous tube, oil burner
ignition), make R1 and R3 approximately equal.
- The series current limiting resistors must be rated to safely handle the
voltage across them as well as their power dissipation. Normal resistors are
usually rated for several hundred V (check the specs) so multiple resistors
in series are required to achieve the required voltage rating.
Alternatively, there are special HV rated resistors designed for this
purpose.
- For the current measuring circuits, additional fixed (R1) and variable
(R2) series resistors have been added in addition to the required shunt
resistor (Rs) to allow a convenient selectrion of shunt resistor value (to
produce a 1 V drop across Rs for full scale current).
The DC circuits
are discussed first. These are generally simpler than those for reading AC
directly and are therefore preferred if a suitable location can be found where
the measurement will be just as meaningful and accurate.
- DC voltage (VDCfs): Use a series resistor equal to: Vfs/Ifs - Rm.
Example: 10 KV full scale using 50 uA movement (negative grounded):
+--+ M1
R1 | v R2 + +---------+ -
+ o-----/\/\-----+-/\/\----------| 0-50 uA |----------+
190M 20M +---------+ _|_
Calibrate 10 KV Full Scale ////
- DC current (IDCfs): Use a shunt resistor equal to: (Im * Rm)/(Ifs - Im).
Example: 1 A full scale using 1 mA movement:
Rs 1 5 W
+ o------+------------------/\/\-----------------+------o -
| |
| +--+ M1 |
| R1 | v R2 + +--------+ - |
+---/\/\---+-/\/\--------| 0-1 mA |-----+
910 100 +--------+
Calibrate 10 A Full Scale
For AC, there are special AC reading meters but these are much
less common than the DC variety. However, where absolute precision and linearity
isn't needed, and an average rather than RMS reading is acceptable, it is a
simple matter to convert a DC meter to respond to AC.
The following circuits for AC voltage and current measurements will actually
read the average, not RMS if components values are calculated using the same
equations as for the DC case. For sinusoids, a simple correction can be made
with the calibrate pot. True RMS readings are left as an exercise for the
student!
- AC voltage (VACfs): Where VACfs is much greater than .7 V (e.g., 100 V), a
a rectifier diode can be added in series with a DC meter. Ignoring the voltage
drop of the diode, the required current limiting resistor will be equal to:
(Vfs/Ifs - Rm)/2.
Example: 500 V (AC) full scale using 100 uA movement:
+--+ M1
D1 R1 | v R2 + +----------+ - R3
AC o----|>|-----/\/\----+-/\/\-----------| 0-100 uA |------/\/\----o AC
1N4007 1.2M 200K +----------+ 1.2M
Calibrate 500 V (AC) Full Scale
Note that since a half wave rectifier is used, the total series
resistance must be half of what it was for the DC measurements.
For high voltages where finding diodes with sufficient ratings is a
problem, use a bridge rectifier - almost any type will do since it doesn't
need to block more than a volt or so. Why? Consider the following:
Example: 10 KV (AC) full scale using 100 uA movement (centertapped HV
transformer):
+--+ D1 M1
R1 | v R2 +--------+ + +----------+ -
AC o----/\/\----+-/\/\------|~ +|-------| 0-100 uA |------+
47M 1M | Little | +----------+ |
R3 Calibrate | Bridge | 10 KV (AC) Full Scale |
AC o----/\/\----------------|~ -|-------------------------+
47M +--------+
Since the voltage across the meter movement itself is probably no more
than a fraction of a volt, this is all the bridge has to worry about! There
will be a dead-zone between +/1 1.5 V or so but who cares on a meter that
reads 10 KV full scale. Ignoring this voltage drop, the required current
limiting resistor will be equal to: (Vfs/Ifs - Rm).
A blocking capacitor can be put in series with the input to this circuit if
there is a DC offset but it must withstand the full voltage (AC peak + DC) and
have a low impedance at the frequency range of interest compared to the sum
R1+R2+R3.
- AC current (VACfs): A series resistor can be placed in the circuit and
then the AC voltage across it can be measured using either of the approaches,
above, or a bridge can be used directly. This time it does need to pass the
full current being measured AND there will be a voltage dead-zone around the
zero crossings of about 1.5 V (however, this won't affect the current reading
linearity. The shunt resistor is equal to: (Im * Rm)/(Ifs - Im).
Example: 100 mA (AC) full scale using 1 mA movement:
+--+ M1
R1 | v R2 + +--------+ -
+---/\/\--+-/\/\------| 0-1 mA |---+
| 940 100 +--------+ |
| Calibrate 100 mA (AC) |
D1 | Full Scale |
+--------+ | Rs |
AC o---------|~ +|---+---/\/\---+-----------------------+
| LV | 10 |
| Bridge | |
AC o---------|~ -|--------------+
+--------+
See the sections: Making
Measurements on HeNe Laser Power supplies and Measurements
of Current and Voltage in Ar/Kr Ion Laser Power Supplies for some
additional comments and examples including safety considerations.
- Back to Sam's
Laser FAQ Table of Contents.
- Back to Amateur
Laser Construction Sub-Table of Contents.
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Laser Types, Information, and Links